Conference Agenda

Overview and details of the sessions of this conference. Please select a date or location to show only sessions at that day or location. Please select a single session for detailed view (with abstracts and downloads if available).

Please note that all times are shown in the time zone of the conference. The current conference time is: 26th Apr 2024, 10:49:28pm CEST

 
 
Session Overview
Session
MS-64: In-situ and time resolved electron crystallography
Time:
Thursday, 19/Aug/2021:
10:20am - 12:45pm

Session Chair: Andrew Alexander Stewart
Session Chair: Eva Olsson
Location: Club H

100 1st floor

Invited: David Flannigan (USA), Maria Batuk (Belgium)


Session Abstract

Nowadays, many measurements are performed in-situ in the electron microscopes. This allows direct measurements of physical and chemical properties of materials and correlation of these properties to microstructure and atomic structure of nano-sized materials. For example: advances such as in-situ electrochemical cells allow direct observation of the behavior of the batteries` materials during charge and discharge cycles.

For all abstracts of the session as prepared for Acta Crystallographica see PDF in Introduction, or individual abstracts below.


Introduction
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Presentations
10:20am - 10:25am
ID: 1795 / MS-64: 1
Introduction
Oral/poster

Introduction to session

Andrew Alexander Stewart, Eva Olsson



10:25am - 10:55am
ID: 1228 / MS-64: 2
Methods and instruments
Invited lecture to session
MS: In-situ and time resolved electron crystallography
Keywords: brownmillerite; TEM; 3D ED; in situ

Following structure evolution of SrFeOx in redox reactions using in situ 3D electron diffraction

Maria Batuk, Daphne Vandemeulebroucke, Joke Hadermann

EMAT, University of Antwerp, Antwerp, Belgium

External Resource:
Video Link


10:55am - 11:25am
ID: 889 / MS-64: 3
Methods and instruments
Invited lecture to session
MS: In-situ and time resolved electron crystallography
Keywords: 4D ultrafast electron microscopy, dynamic TEM, automation, synchronization, radiation damage

Time-resolved TEM beyond fast detectors

David J. Flannigan, Jialiang Chen, Wyatt Curtis, Daniel X. Du, Paige E. Engen, Elisah J. VandenBussche, Yichao Zhang

Department of Chemical Engineering and Materials Science, University of Minnesota, 421 Washington Avenue SE, Minneapolis, Minnesota 55455, United States of America

External Resource:
Video Link


11:25am - 11:50am
ID: 476 / MS-64: 4
Bursary application
Oral/poster
MS: High pressure crystallography, Solid state reactions and dynamics, In-situ and time resolved electron crystallography
Posters only: Structure and phase transitions in advanced materials, Methods, instrumentation (if it does not fit to any specific topics)
Keywords: X-ray diffraction, time-resolved experiments, crystals under dynamic loads

Time resolved x-ray diffraction studies of prospective crystalline materials under dynamic ultrasonic loads

Yan Eliovich1,2, Anton Targonskiy1,2, Alexander Blagov1,2, Yuri Pisarevsky1,2, Valentin Akkuratov1,2, Andrei Protsenko1,2, Michail Kovalchuk1,2

1FSRC “Crystallography and photonics” RAS, Moscow, Russian Federation; 2NRC "Kurchatov Institute", Moscow, Russian Federation

Bibliography
1.X-ray acoustic diffractometry for the control of electronic components and materials. A.V. Targonsky, A.E. Blagov, Yu. V. Pisarevski, P.A. Prosekov, I.A. Eliovich, M.V. Kovalchuk. Fundamental problems of electronic instrumentation. 2013. Vol. 13. № 1. P. 32.
2.NEW OPPORTUNITIES OF X-RAY ACOUSTOOPTICS. A.E. Blagov, A.V. Targonsky, Yu. V. Pisarevski, P.A. Prosekov, I.A. Eliovich, M.V. Kovalchuk. Bulletin of the Russian Foundation for Basic Research. 2014. Vol 2 (82). P. 18.
3.Measurement of rocking curves of crystals using an acoustically tunable monochromator. A.E. Blagov, P.A. Prosekov, A.V. Targonskii, Ya.A. Eliovich. Crystallography Reports. 2015. Vol. 60. №2. P.167.
4.An electromechanical x-ray optical element based on a hysteresis-free monolithic bimorph crystal. A.E. Blagov, A.S. Bykov, I.V. Kubasov, M.D. Malinkovich, Yu.V. Pisarevskii, A.V. Targonskii, I.A. Eliovich, M.V. Kovalchuk. 2016. Vol. 59. №5. P.782.
5.Evolution of X-ray rocking curves for paratellurite and lithium fluoride crystals under intense ultrasound. A.E. Blagov, Yu.V. Pisarevskii, A.V. Targonskii, Ya.A. Eliovich, M.V. Koval’chuk. 2017. Physics of the Solid State. Vol. 59. №5. P.973.
6.Development of methods for ultrasonic scanning of X-ray wavelength. A.E. Blagov, Yu.V. Pisarevskii, P.A. Prosekov, A.V. Targonskii, Ya.A. Eliovich, A.I. Protsenko, M.V. Koval’chuk. 2017. Crystallography ReportsVol. 62. № 6. P.831.
7.Investigations of the Growth Processes of Bismuth-Germanate Crystals (Bi12GeO20) from the Melt using the X-Ray Diffraction Characteristics of Natural Lateral Faces. A.A. Mololkin, A.I. Protsenko, A.E. Blagov, A.V. Vinogradov, V.A. Lomonov, Yu.V. Pisarevskii, A.V. Targonskii, Ya.A Eliovich. Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques. 2018. Vol. 12. №1. P.69.
8.Rocking Curve Measurement for Deformed Crystals Using an Adaptive X-Ray Optical Bending Monochromator. I.A. Eliovich, V.I. Akkuratov, A.V. Targonskii, A.E. Blagov. Crystallography Reports. 2018. Vol. 63. №5. P.724.
9.Crystal growth and optical properties of Ca3TaGa3Si2O14 single crystals. O.A. Buzanov, N.S. Kozlova, A.P. Kozlova, E.V. Zabelina, A.E. Blagov, I.A. Eliovich, A.G. Kulikov, A.V. Targonskiy. Japanese Journal of Applied Physics. 2018. Vo. 57. 11UD08.
10.LiNbO3-based bimorph piezoactuator for fast X-ray experiments: Static and quasistatic modes. A. Kulikov, A. Blagov, N. Marchenkov, A. Targonsky, Ya. Eliovich, Yu. Pisarevsky, M. Kovalchuk. Sensors and Actuators A: Physical. 2019. Vol. 291. P.68.
11.LiNbO3-based bimorph piezoactuator for fast X-Ray experiments: Resonant mode. N. Marchenkov, A. Kulikov, A. Targonsky, Ya. Eliovich, Yu. Pisarevsky, A. Seregin, A. Blagov, M. Kovalchuk. Sensors and Actuators A: Physical. 2019. Vo. 293. P.48.
12.Multiple-Wave Interaction of X-Rays in a Paratellurite Crystal under Excitation of Ultrasonic Vibrations. Ya.A. Eliovich, A.V. Targonskii, A.N. Darinskii, P.A. Prosekov, Yu.V. Pisarevsky, A.E. Blagov, V.I. Akkuratov, V.A. Lomonov, V.R. Kocharyan, A.R. Mkrtchyan, M.V. Kovalchuk. Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques. 2019. Vol.13. №4. P.570
13.Distribution of Deformations in the Oscillating X-Ray Acoustic Element Based on the X-Cut Quartz Crystal. Journal of Contemporary Physics. A.R. Mkrtchyan, A.E. Blagov, V.R. Kocharyan, A.G. Kulikov, A.E. Movsisyan, T.R. Muradyan, A.V. Targonsky, Ya.A. Eliovich, A.N. Darinski, Yu.V. Pisarevski, M.V. Kovalchuk. 2019. Vol. 54. №2. P.210.
External Resource:
Video Link


11:50am - 12:15pm
ID: 824 / MS-64: 5
Methods and instruments
Oral/poster
MS: In-situ and time resolved electron crystallography
Keywords: crystal discovery; solid-state precipitates; in situ transmission electron microscopy; atomistic simulations

Discovering and transforming precipitate phases in aluminium alloys using in situ transmission electron microscopy

Laure Bourgeois1,2, Zezhong Zhang3,4, Yong Zhang2, Xiaofen Tan2, Yiqiang Chen5, Matthew Weyland1,2, Philip N.H. Nakashima2, Nikhil V. Medhekar2

1Monash Centre for Electron Microscopy, Monash University, Australia; 2Department of Materials Science and Engineering, Monash University, Australia; 3Electron Microscopy for Materials Research, University of Antwerp, Belgium; 4Department of Materials, University of Oxford, UK; 5Thermofisher Scientific, The Netherlands

External Resource:
Video Link


12:15pm - 12:40pm
ID: 727 / MS-64: 6
Bursary application
Oral/poster
MS: Dynamic frameworks, In-situ and time resolved electron crystallography, Application of electron crystallography to functional materials
Posters only: Porous materials
Keywords: ADPs, flexibility, MOFs, cRED

Elucidation of Linker Motion in Metal-Organic Frameworks by Three-Dimensional Electron Diffraction

Laura Samperisi1, Aleksander Jaworski1, Gurpreet Kaur1, Karl P. Lillerud2, Xiaodong Zou1, Zhehao Huang1

1stockholm university, stockholm, Sweden; 2University of Oslo, Oslo, Norway

Bibliography
M. O. Cichocka, Z. Liang, D. Feng, S. Back, S. Siahrostami, X. Wang, L. Samperisi,Y. Sun,H. Xu,N. Hedin,H. Zheng, X.Zou, H.-C. Zhou, Z. Huang, J. Am. Chem. Soc. 2020, 142, 15386– 15395.
External Resource:
Video Link


 
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